Abstract
A dipyridylamine ligand with a pendant pyrrole ( N-(3- N, N′-bis(2-pyridyl)propylamino)pyrrole, PPP) and its corresponding rhenium(I) complex, Re(CO) 3(κ 2- N, N-PPP)Cl, were synthesized. The structure of Re(CO) 3(κ 2- N, N-PPP)Cl was determined by X-ray crystallography. Electrochemical polymerization of the pyrrole moiety resulted in the immobilization of poly[Re(CO) 3(κ 2- N, N-PPP)Cl] film onto a glassy carbon electrode, which exhibited electrocatalytic activity for the reduction of CO 2 to CO.
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