Abstract
Oxidations of dimethyl sulfoxide, toluene, and p‐xylene at pure electrodes were determined to be under extreme kinetic control with values of the apparent heterogeneous rate constant . However, a significant increase in was observed at acetate‐doped electrodes in 1M . X‐ray diffraction data indicated the films retained the slightly distorted rutile structure of the β‐form of the pure . Catalysis of the anodic discharge of to produce adsorbed hydroxyl radicals is concluded to account for the enhanced catalytic activity of the films for the anodic oxygen transfer reactions in .
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