Abstract
The new chiral diphosphine 2 was synthesized from mucochloric acid. The structure of the NiI2-complex 7 was determined by single crystal X-ray analysis. 7 crystallizes in the orthorhombic space group P212121. The lattice constants (at 180 K) are: a = 914.1(2); b = 1422.0(3); c = 4112.5(10) pm.
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