Abstract
Synthetic efforts toward the tricyclic core of (±)-toxicodenane A are reported. This strategy takes advantage of the Feist-Benary furan annulation, Achmatowicz oxidative rearrangement, and oxidopyrylium-based [5+2] cycloaddition to access a key tetracyclic intermediate. This work provides a foundation that can be utilized toward the total synthesis of the natural product.
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