Abstract
Our studies of the TIBAL-promoted Claisen rearrangement reaction and ring-closing metathesis (RCM) resulted in the development of an efficient synthetic route to polyfunctional seven-membered carbasugar synthons from d-arabinose. Moreover, the construction of 8-oxa-bicyclo[3.2.1]octane derivatives 10 and 13 was achieved by BCl 3 or iodide-promoted intramolecular electrophilic addition reactions, which were regio- and stereoselective.
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