Effects of Magnesium Variation and Heat Treatment on Mechanical and Micro-Structural Properties of Ductile Cast Iron

Abstract

The effects of magnesium variation and austempering heat treatment on mechanical and microstructural properties of ductile iron produced using the rotary furnace were investigated. Varied quantity of magnesium-ferrosilicon in the range of 0.03 % to 0.06 % were used as nodulirizer to treat 4 kg mass of molten metal per ladle by sandwich process and poured into sand mould. Mechanical test (tensile, hardness, fatigue, impact and wear) and micro-structural examinations were carried out on the four samples produced. Samples C and D of 0.056% and 0.061% magnesium showed an improvement in their micro-structural properties due to the presence of more graphite nodules. Hence, they were observed to have exhibited better tensile strength of 598.07MPa and 609.03MPa. The fatigue strength also increased to 501.91MPa and 509.27MPa respectively. These two samples were further subjected to austempering heat treatment by heating to 850ºC for austenitization and soaked for homogenization for one hour at the temperature before quickly transferred into a salt bath of 50 % NaNO3 : 50 % NaCl maintained at 3600C and quenched for transformation for 1 hour before finally air cooled. Mechanical tests and micro-structural examinations were thereafter carried out. Sample C had an outstanding increase in tensile strength, from 598.07MPa to 891.22MPa, while specimen D increased from 609.03MPa to 898.76MPa. The results of abrasion test indicated that samples C and D had abrasion resistance increase from 2.20×10¹¹m² and 2.39×10¹¹m² to 2.35×10¹¹m² and 2.68×10¹¹ m² respectively after austempering. There were also relative increase in fatigue resistance and impact toughness for the two samples but with relative reduction in hardness from 47.7 to 44.2 and 50.3 to 47.4.