Effects of intermediate annealing on the microstructure and transport properties of Bi-2223 wires and tapes

Abstract

Monofilament and 37-filamentary Bi-2223 tapes were fabricated by powder in tube (PIT) process. And the mono-filamentary wires were drawn from ϕ12mm to hexagon 1.51 mm with one and three times intermediate annealing, respectively. The influences of different intermediate annealing times on the core density, morphology and transport properties of Bi-2223 wires and tapes were systematically investigated. It was noticed that the density and the Vickers micro-hardness values of superconducting core on the cross-section of one time annealing wires were higher than those of three times annealing wires. Meanwhile, it was observed that the Ag/oxide core interfaces of the wire with one time annealing were more smooth than those of the three times annealing wire. With the intermediate annealing time decreasing from three to one, the critical current density Jc increased from 17.9 kA/cm2 to 20.5 kA/cm2. And the enhancement of Jc-B properties suggests the improvement of intergrain connections due to the increasing core density. Meanwhile one time annealing procedure was used to Ag-Au sheathed tape, Jc reached 16.3 kA/cm2, this value was also higher than those traditional wires in our previous experiments, which suggests that the decreasing of annealing times during drawing process is also effective in AgAu sheath tapes for the enhancement of current capacity.