Abstract

The choice of melting technique is crucial for controlling the purity of a superalloy, which is especially important because purity has come to limit progress in the superalloy field. In this study, double- and triple-melting techniques were used to refine the GH4738 superalloy. Elemental analyses, inductively coupled plasma-atomic emission spectroscopy, X-ray diffraction analysis, scanning electron microscopy with energy-dispersive spectroscopy, high-temperature cupping machine, high-temperature fatigue testing machine, and Image-Pro Plus software were used to analyze and compare the contents of specific elements, the types and sizes of inclusions, the mechanical properties, and the probabilities of white spot formation using the two melting techniques. The effects of the different melting processes on the purity of the superalloy were systematically studied. In terms of controlling the presence of impurities, the triple-melting process resulted in lower levels of harmful N, S, and O impurities in the superalloy, the triple-melted superalloy also contained fewer types of inclusion of smaller sizes and in smaller amounts than the double-melted alloy. Triple melting also promotes tensile strength and fatigue life, and minimizes the probability of forming defects in the superalloy.

Highlights

  • Superalloys, owing to their excellent high-temperature strengths and good resistance to oxidation, fatigue, and creep deformation [1,2,3], have emerged as materials for components that operate at high temperatures in the fields of aerospace and aviation engineering

  • It is difficult to precisely determine the melting technique best suited for the preparation of a high-purity superalloy, which limits further improvements in superalloy performance

  • The results reveal that the chemical compositions of the superalloys produced by the two different smelting processes meet technical requirements, but their elemental compositions and evolutions differ markedly

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Summary

Introduction

Superalloys, owing to their excellent high-temperature strengths and good resistance to oxidation, fatigue, and creep deformation [1,2,3], have emerged as materials for components that operate at high temperatures in the fields of aerospace and aviation engineering. These include turbine disks and blades, and combustion chambers in aerospace engines; these alloys enjoy reputations as “cornerstones for advanced engines” [4,5,6]. It is difficult to precisely determine the melting technique best suited for the preparation of a high-purity superalloy, which limits further improvements in superalloy performance To overcome this problem, the effects of different melting techniques on superalloy purity should be studied. This research serves as a guide for the selection of appropriate melting techniques for improving superalloy purity; in this sense, it provides a theoretical foundation

Melting
Preparation and Testing
Chemical-Composition Analysis
XRD Analyses
Inclusion Characteristics and Their Formation Mechanism
Analysis of Mechanical Properties
Analysis of White-Spot Formation Probability
Conclusions
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