Abstract
The effects of fluid density on the voltammetry of ferrocene in CO 2 -based fluids have been investigated with microelectrodes coated with Nafion films. Voltammograms have been obtained in water-modified CO 2 over a range of temperatures and pressures spanning the critical point of CO 2 (T=31.4 o C, 1073 psi). Thus, the voltammetry of ferrocene has been examined in both subcritical and supercritical fluids. In order to qualitatively investigate the effect of fluid density on the partition coefficient of ferrocene between the film and fluid, the absorbance due to ferrocene in the fluid was also measured
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