Abstract

The effect of ultrasonic nanocrystal surface modification (UNSM) on the fatigue behavior of Ti6Al4V (TC4) in simulated body fluid (SBF) was investigated. UNSM with the condition of a static load of 25 N, vibration amplitude of 30 μm and 36,000 strikes per unit produced about 35 μm surface severe plastic deformation (SPD) layers on the TC4 specimens. One group was treated with a hybrid surface treatment (UNSM + TiN film). UNSM technique improves the micro hardness and the compressive residual stress. The surface roughness is increased slightly, but it can be remarkably improved by the TiN film. The fatigue strength of TC4 is improved by about 7.9% after UNSM. Though the current density of corrosion is increased and the pitting corrosion is accelerated, UNSM still improved the fatigue strength of TC4 after pre-soaking in SBF by 10.8%. Interior cracks initiate at the deformed carbide and oxide inclusions due to the ultrasonic impacts of UNSM. Corrosion products are always observed at the edge of fracture surface to both interior cracks and surface cracks. Coating a TiN film on the UNSMed surface helps to improve the whole properties of TC4 further.

Highlights

  • The surface condition is of particular importance to the fatigue properties of metals

  • The mechanical processes include surface mechanical attrition treatment (SMAT) [3,4], ultrasonic shot peening (USSP) [5], laser shock peening (LSP) [6], ultrasonic surface rolling processing (USRP) [7], ultrasonic cold forging technology (UCFT) [8], and so on. These techniques help to transform the coarse grains of a bulk material into nanosized grains by surface severe plastic deformation (SPD)

  • The hardness of the surface after ultrasonic nanocrystal surface modification (UNSM) was increased by 22.6% compared with that of initial TC4 specimen (IS)

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Summary

Introduction

The surface condition is of particular importance to the fatigue properties of metals. The mechanical processes include surface mechanical attrition treatment (SMAT) [3,4], ultrasonic shot peening (USSP) [5], laser shock peening (LSP) [6], ultrasonic surface rolling processing (USRP) [7], ultrasonic cold forging technology (UCFT) [8], and so on These techniques help to transform the coarse grains of a bulk material into nanosized grains by surface severe plastic deformation (SPD). The corrosion fatigue properties of titanium alloys in body fluid should be studied. Bioactive membranes such as TiO, TiN, ZrO2 , hydroxyapatite and diamond-like carbon films have been developed onto titanium alloys to improve the wear ability and the adhesion of cells [22,23,24,25]. A hybrid surface treatment (UNSM + TiN film) was prepared as a comparision group

Experimental Procedures
Observation of the Severe
The microstructure
Micro Vickers Hardness and Residual Stress Distrubution
Distribution of of compressive andmicro microVickers
Surface
Surface roughness of TC4 after nanocrystal modification
Corrosion Resistance
The ofand
Specimens thatnot did not encounter
S-N in SBF
Conclusions
Full Text
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