Abstract
Rapidly solidified samples of Nd9.5Fe84.5B6 with and without 3 at. % TiC were prepared by melt spinning and melt extraction and then annealed in vacuum (3×10−6 Torr) at temperatures from 600 to 750 °C. For alloys melt spun under similar conditions, the overquenched state was achieved at wheel speeds >10 m/s for the TiC added alloy while >20 m/s was necessary without TiC. The overquenched samples contained a smaller fraction of α-Fe in smaller grains than the undercooled samples where Fe dendrites formed near the free surface during solidification. These Fe dendrites were not removed by annealing. In addition, large orientated 2-14-1 grains nucleated on the Fe dendrites. This combination is detrimental to the magnetic properties. The addition of TiC results in improved control of the microstructure over a larger fraction of the ribbon volume enhancing the magnetic properties.
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