Abstract
The presence of a constant electric field (300 kV m–1) and variation of CO2 concentration in the fluid affected the morphology of ZnO nanocrystals and the internal structure of ZnO layer obtained on interacting zinc anode with supercritical H2O/CO2 at 673 K and 35 MPa. The electric field favors the formation of zinc oxalate and carbonate, the thermal decomposition of which forms the pore structured of ZnO. Moreover, a fraction of elongated nanocrystals in the surface layer of ZnO is increased due to the action of the electric field.
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