Abstract

Heating by absorption of light is a commonly used technique to ensure a fast temperature increase of metallic samples. The rate of heating when using optical heating depends critically on the absorption of light by a sample. Here, the reflection and scattering of light from UV to IR by surfaces with different roughness of iron-based alloy samples (Fe, 1 wt-% Cr) is investigated. A combination of ellipsometric and optical scattering measurements is used to derive a simplified parametrisation which can be used to obtain the absorption of light from random rough metal surfaces, as prepared through conventional grinding and polishing techniques. By modelling the ellipsometric data of the flattest sample, the pseudodielectric function of the base material is derived. Describing an increased roughness by a Maxwell-Garnett model does not yield a reflectivity which follows the experimentally observed sum of scattered and reflected intensities. Therefore, a simple approach is introduced, based on multiple reflections, where the number of reflections depends on the surface roughness. This approach describes the data well, and is subsequently used to estimate the fraction of absorbed energy. Using numerical modelling, the effect on the heating rate is investigated. A numerical example is analysed, which shows that slight changes in roughness may result in big differences of the energy input into a metallic sample, with consequences on the achieved temperatures. Though the model oversimplifies reality, it provides a physically intuitive approach to estimate trends.

Highlights

  • The search for stable materials during fast temperature changes or thermal cycling conditions is one of the biggest challenges in modern alloy design

  • A combination of ellipsometric and optical scattering measurements is used to derive a simplified parametrisation which can be used to obtain the absorption of light from random rough metal surfaces, as prepared through conventional grinding and polishing techniques

  • A numerical example is analysed, which shows that slight changes in roughness may result in big differences of the energy input into a metallic sample, with consequences on the achieved temperatures

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Summary

Blumich

Max-Planck-Institut fur Eisenforschung GmbH, Max-Planck-Straße 1, 40237 Dusseldorf, Germany Christian Doppler Laboratory for Diffusion and Segregation Phenomena during the Production of High Strength Steel Sheets Max-Planck-Institut fur Eisenforschung GmbH, Max-Planck-Straße 1, 40237 Dusseldorf, Germany. Heating by absorption of light is a commonly used technique to ensure a fast temperature increase of metallic samples. The reflection and scattering of light from UV to IR by surfaces with different roughness of iron-based alloy samples (Fe, 1 wt-% Cr) is investigated. A combination of ellipsometric and optical scattering measurements is used to derive a simplified parametrisation which can be used to obtain the absorption of light from random rough metal surfaces, as prepared through conventional grinding and polishing techniques. A simple approach is introduced, based on multiple reflections, where the number of reflections depends on the surface roughness. This approach describes the data well, and is subsequently used to estimate the fraction of absorbed energy.

INTRODUCTION
EXPERIMENTAL
Surface Roughness
Reflection and Scattering Measurements
Consequences for Optical Heating
CONCLUSION
A Model Parameters and Statistical Data for Reflectivity Modelling
C Temperature Difference during a Heating Cycle
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