Abstract
In the present work, we have investigated the formation of nanostructured oxide layers by anodic oxidation on different surface finished (mirror finished, 600 and 400 grit polished) nickel–titanium alloy (Ni–Ti) in electrolyte solution containing ethylene glycol and NH4F. The anodized surface has been characterized by field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS) and X‐ray photoelectron spectroscopy (XPS). The corrosion behaviors of the Ni–Ti substrate and anodized samples have been investigated by electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization in simulated body fluid (Hanks' solution). The results show that the native oxide on the substrate is replaced by nanostructures through anodization process. XPS of Ni–Ti substrate shows the presence of Ni0, NiO, Ti0 and TiO2 species, whereas Ni2O3 and Ni(OH)2 and TiO2 are observed in the samples after anodization. Corrosion resistance of the anodized sample is comparable with that of the untreated sample. Copyright © 2016 John Wiley & Sons, Ltd.
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