Abstract

The impacts of rolling temperature on phase transformations and mechanical properties were investigated for AISI 316LN austenitic stainless steel subjected to rolling at cryogenic and room temperatures. The microstructure evolution and the mechanical properties were investigated by means of optical, scanning, and transmission electron microscopy, an X-ray diffractometer, microhardness tester, and tensile testing system. Results showed that strain-induced martensitic transformation occurred at both deformation temperatures, and the martensite volume fraction increased with the deformation. Compared with room temperature rolling, cryorolling substantially enhanced the martensite transformation rate. At 50% deformation, it yielded the same fraction as the room temperature counterpart at 90% strain, while at 70%, it totally transformed the austenite to martensite. The strength and hardness of the stainless steel increased remarkably with the deformation, but the corresponding elongation decreased dramatically. Meanwhile, the tensile fracture morphology changed from a typical ductile rupture to a mixture of ductile and quasi-cleavage fracture. The phase transformation and deformation mechanisms differed at two temperatures, with the martensite deformation contributing to the former, and austenite deformation to the latter. Orientations between the transformed martensite and its parent phase followed the K–S (Kurdjumov–Sachs) relationship.

Highlights

  • As one of the key stainless steels (SSs), 316LN austenitic SSs (ASS) possess outstanding anticorrosion and antioxidation merits, yet are widely used in various fields such as petroleum, chemical industry, and nuclear power plants [1,2]

  • The total phase transformation could not be reached through room temperature rolling

  • The results revealed that cryorolled deformation did not change the way of new phase generation, but affected the transition dynamics

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Summary

Introduction

As one of the key stainless steels (SSs), 316LN austenitic SSs (ASS) possess outstanding anticorrosion and antioxidation merits, yet are widely used in various fields such as petroleum, chemical industry, and nuclear power plants [1,2]. The rather low yield strength, only 200 MPa after solid solution treatment, demands additional treatments to broaden its application fields. It has been noticed that its mechanical properties can be enhanced by grain refinement, phase transformation strengthening, and work hardening [3,4,5]. High ductility and high yield strength have been introduced into the treated ASS. During cold rolling, the stable ASS (e.g., 310S ASS) can maintain the austenitic structure after deformation [6,7]. As for the meta-stable ASS such as 304 and 316

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