Abstract

Compacts, made from a microwave-plasma-synthesized Fe nanopowder, were sintered under H 2 at increasing temperatures. Despite its initial nanosize, we did not observe any enhanced, low-temperature sintering behavior with the powder. Using FESEM, XRD, and BET surface area, we found that the primary nanoparticles are aggregated into micrometer-sized dendritic structures that hinder sintering and densification.

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