Effect of plasma treatment on the wettability of elastomeric impression materials

Abstract

This study investigated the effect of "plasma treatment" on the wettability of impression materials and void formation in die stone casts. Four addition reaction silicones, one condensation reaction silicone, and one polyether impression material were used. Wettability was determined before and after plasma treatment by contact angle registration of a saturated aqueous solution of calcium sulfate (CaSO4) on flat surfaces made from the tested impression materials. Two groups of surfaces were used for each material. The surfaces in one of the groups were exposed to saliva for 5 minutes. The same impression materials were used to produce four groups of die stone casts from a master die. Two groups were produced from impressions that had been exposed to milk. One group from the exposed and one from the bare surfaces were plasma-treated before pouring. Voids in the stone casts were counted under a stereoscopic microscope. The results indicated that after plasma treatment, the drop of CaSO4 solution completely spread over the addition type silicone surfaces. The corresponding die stone casts were found to be void free. It was concluded that plasma treatment produced high-energy impression surfaces that result in void-free die stone casts from the addition type silicone materials.