Abstract

Titanium dioxide (TiO 2) nanopowders were successfully prepared by thermal processing of the precursor of titanium hydroxide, urea and sodium acid carbonate (NaHCO 3). The products were characterized by X-ray diffractometry, scanning electron microscopy, transmission electron microscopy and X-ray photoelectron spectroscopy. The results show that NaHCO 3 has a certain effect on the average crystallite size and dispersity of TiO 2 nanopowders, at the same time other phases (Na 2SO 4 and Na 2CO 3) will be introduced. However, Na 2SO 4 has distinctive intercalation ability and catalytic activity. TiO 2 (anatase) powders can be prepared at −600 °C for 2 h with addition of 2–10 wt% NaHCO 3, and the average crystallite size is 20.0–22.3 nm. The surface of the sample mainly consists of Ti, O, C, Na and S five species elements.

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.