Effect of mixture composition, nanoparticle density and sound intensity on mixing quality of nanopowders

Abstract

The present work is focused on the characterization of nanoparticles mixing under sound assisted fluidization. In particular, the effects of mixture composition, primary particles density and sound intensity on the mixing quality have been pointed out. The effect of the relative amount of the two powders has been investigated using Al 2O 3 and Fe 2O 3 nanopowders and carrying out tests at fixed acoustic field (130 dB–120 Hz) and varying the mixture composition (17, 50 and 77 wt% of Fe 2O 3). Whereas, the effect of nanoparticles density has been studied performing mixing tests between two denser powders, ZrO 2 and CuO, at fixed mixture composition (50 wt% of ZrO 2) and acoustic field (130 dB–120 Hz), and comparing the results with those obtained with the two lighter powders (Al 2O 3 and Fe 2O 3). Moreover, tests between ZrO 2 and CuO have also been carried out at different sound intensities (130 and 140 dB), at a fixed frequency and mixture composition, in order to highlight the influence of SPL. Both the “global” and the “local” mixing between two different powders have been investigated by means of the Scanning Electron Microscopy with X-ray microanalysis (SEM/EDS) analysis of captured samples, in order to obtain the time dependence of the mixing degree, its asymptotic value and the mixing characteristic time.