Abstract
A powder mixture of Al/ZrO2/H3BO3 system was mechanically milled under argon in a high-energy planetary mill at different speeds. The XRD and DSC analyses of the as-synthesized samples show that milling operation affects the mechanism, efficiency, and ignition temperature of combustion behavior of the system. XRD analysis of the as-milled samples shows that low-speed milling does not change the phases presented in the sample, while high-speed milling (350, 450 rpm) has led to the formation of new intermetallic phases. This confirms that some reactions between reactants have occurred during high-speed milling.
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