Abstract

The microstructure and microhardness of X70 pipeline steel were investigated after conducting different processing routes. The microstructure was characterized using optical and electron microscopy. Scanning electron microscopy equipped with electron backscattered diffraction (EBSD) and transmission electron microscopy techniques were applied for investigation of different thermal processing treatment conditions. Mechanical properties were characterized by a microhardness tester. The results show that the microstructure mainly consists of granular bainite, acicular ferrite and a small amount of M/A constituents under hot rolling states. There are many dislocations inside the acicular ferrite. The thermal simulation experiments show that the microstructure becomes homogeneous with the increase in cooling rate. The acicular ferrite morphology becomes fine and uniform, and the content of M/A constituents increases at the same compression amount. The compression gives rise to the accumulated strain and stored energy, which accelerate the transformation of acicular ferrite and refine the microstructure of the pipeline steel. The microhardness rises with the increase in deformation ratio and cooling rate. The microstructure of the pipeline steel subjected to the isothermal quenching process is ultrafine ferrite and M/A islands. When the isothermal quenching temperature reaches 550 °C, a small amount of upper bainite appears in the microstructure. With the increase in isothermal quenching temperature, the microhardness decreases. Acicular ferrite is a better candidate microstructure than ultrafine ferrite for the pipeline steels.

Highlights

  • Pipeline steel is mainly used in offshore oil and gas extraction and transmission, which has comprehensive mechanical properties such as high strength [1], good impact toughness [2,3], and high corrosion resistance [4,5,6]

  • Conventional thermomechanical control processing (TMCP) is a commonly used technology for manufacturing pipeline steel products that can control the transformation temperature and inhibition of the grain growth [21,22]. These previous results suggest that the microstructure is mainly composed of the acicular ferrite (AF), quasi-polygonal ferrite (QF), polygonal ferrite, and even some dispersed martensite/austenite (M/A) constituent in the pipeline steels [10]

  • The acicular ferrite plays a significant role in improving the mechanical properties of pipeline steels [23], providing high strength and excellent low-temperature toughness [24,25]

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Summary

Introduction

Pipeline steel is mainly used in offshore oil and gas extraction and transmission, which has comprehensive mechanical properties such as high strength [1], good impact toughness [2,3], and high corrosion resistance [4,5,6]. Conventional thermomechanical control processing (TMCP) is a commonly used technology for manufacturing pipeline steel products that can control the transformation temperature and inhibition of the grain growth [21,22] These previous results suggest that the microstructure is mainly composed of the acicular ferrite (AF), quasi-polygonal ferrite (QF), polygonal ferrite, and even some dispersed martensite/austenite (M/A) constituent in the pipeline steels [10]. The acicular ferrite plays a significant role in improving the mechanical properties of pipeline steels [23], providing high strength and excellent low-temperature toughness [24,25]. It has been established in previous research that the acicular ferrite is a non-equiaxed phase with high dislocation density [25]. The metallographic characteristics and classification of the acicular ferrite are still controversial and cause disagreements as regards pipeline steel

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