Abstract

The present work deals with the effect of iron intermetallics on the microstructure and mechanical properties of Al-7% Si alloys. Two different iron additions were made, 0.6% Fe and 2% Fe, to study the effect of iron intermetallics on Al-Si alloys.Microstructure property correlations were carried out using SEM-EDS and tensile testing of alloys. Microstructure results show that the rise in iron content significantly increased the average size, thickness and number of intermetallic particles in the alloys. Nano-indentation study shows that the iron intermetallics are too brittle compared with the primary aluminium. Moreover, the hardness and Young’s modulus of iron intermetallics are higher than those of primary aluminium.Tensile test results show that there is no significant difference in strength levels between Al-7%Si and Al-7Si-0.6Fe alloys. However, an increase in iron from 0.6% to 2% resulted in a significant decrease in tensile strength and elongation of the alloys. Two-dimensional SEM studies suggest that the increased number of needle-shaped β-phase intermetallic particles formed because of increased amounts of Fe could be the reason for early failure of the alloy. To further understand the early failure of iron-containing alloys, the fractured tensile specimens were studied using the 3D x-ray tomography technique. XCT results show that the failure in tensile testing of 2% Fe alloy was not mainly due to breaking of brittle β-phase intermetallic particles, but due to the morphology and particle-matrix interface debonding. XCT shows that the needle-shaped particles are long, sharp-edged platelets in 3D, which act as stress raisers for crack initiation and propagation along the interphase.

Highlights

  • Recycling of aluminium and aluminium alloys is a topic of interest in automotive and aerospace industries because of the economic and environmental benefits associated with it.[1]

  • This shows that the increase in iron content from 0.6% Fe to 2% Fe resulted in a significant increase in the volume fraction of iron intermetallics in the alloy

  • Nanoindentation studies show that the iron intermetallic particles are hard and brittle compared with the primary aluminium

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Summary

INTRODUCTION

Recycling of aluminium and aluminium alloys is a topic of interest in automotive and aerospace industries because of the economic and environmental benefits associated with it.[1]. Three-dimensional analysis later showed that the b phase is platelet shaped, but was misinterpreted as needle shaped in 2D observations.[6] The b-phase intermetallic particles were considered more harmful in deteriorating the mechanical properties of aluminium alloys.[7] Several studies have been carried out to understand the effect of intermetallics on the mechanical properties of Al-Si alloys.[8,9,10,11] most of these studies show the effect of intermetallics on mechanical properties only by considering 2D microstructural observations. We present the effect of iron content on the microstructure and mechanical properties of Al7 wt.% Si alloy and Al-7 wt.% Si-2 wt.% Fe alloy using high-resolution electron microscopy imaging and 3D x-ray computed tomography (XCT) investigation

Alloy Preparation
Microstructural Characterisation
Mechanical Property Characterisation
Zeiss Versa
RESULTS
CONCLUSION
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