Effect of different surface treatments on the composite–composite repair bond strength

Abstract

The aim of this study was to investigate the effect of different mechanical and adhesive treatments on the bond strength between pre-existing composite and repair composite using two aging times of the composite to be repaired. Standardized cylinders were made of a microhybrid composite (Spectrum TPH) and stored in saline at 37 degrees C for 24 h (n = 140) or 6 months (n = 140). Three types of mechanical roughening were selected: diamond-coated bur followed by phosphoric acid etching, mini sandblaster with 50-microm aluminum oxide powder, and 30-microm silica-coated aluminum oxide powder (CoJet Sand), respectively. Adhesive treatment was performed with the components of a multi-step bonding system (OptiBond FL) or with a one-bottle primer-adhesive (Excite). In the CoJet Sand group, the effect of a silane coupling agent (Monobond-S) was also investigated. The repair composite (Spectrum TPH) was applied into a mould in three layers of 1 mm, each separately light-cured for 40 s. Repair tensile bond strengths were determined after 24-h storage. Mechanical and adhesive treatment had significant effects on repair bond strength (P < 0.001). The age of the pre-existing composite had no significant effect (P = 0.955). With one exception (CoJet Sand/OptiBond FL Adhesive), adhesive treatments significantly increased repair bond strengths to 6-month-old composite when compared to the controls without adhesive. Adhesive treatment of the mechanically roughened composite is essential for achieving acceptable repair bond strengths. The more complicated use of silica-coated particles for sandblasting followed by a silane coupling agent had no advantage over common bonding systems.