Abstract
Environmentally friendly methods for the synthesis of T8 H were developed. A combination of triethoxysilane (TES), concentrated HCl aqueous solution, and FeCl3 produced T8 H with almost the same yield as the previously known methods. We also found that HNO3 could be used instead of HCl, resulting in a similar yield. No toxic gases were generated during the reaction with HNO3. Additionally, the synthesis of T8 H based on TES did not generate dangerous substances such as hydrogen chloride and methanol, unlike when trichlorosilane or trimethoxysilane are used. Therefore, our new method for the synthesis of T8 H is considered to be safer, although the yield is the same as the conventional methods.
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