Abstract
In the title molecule, C25H19NO2, the furyl ring is twisted by 46.3 (1)° with respect to the phenylene ring bearing the amido group. In the stilbene unit, the two phenylene rings (i.e. the rings connected through the –CH=CH– fragment) are twisted by 59.2 (1)°; in the biphenylene unit, the two benzene rings are twisted by 35.5 (1)°. In the crystal structure, molecules are linked by an N—H⋯Oamido hydrogen bond into a zigzag chain running along the c axis.
Highlights
In the title molecule, C25H19NO2, the furyl ring is twisted by 46.3 (1) with respect to the phenylene ring bearing the amido group
The two phenylene rings are twisted by 59.2 (1); in the biphenylene unit, the two benzene rings are twisted by 35.5 (1)
Molecules are linked by an N—HÁ Á ÁOamido hydrogen bond into a zigzag chain running along the c axis
Summary
Key indicators: single-crystal X-ray study; T = 100 K; mean (C–C) = 0.002 A; R factor = 0.039; wR factor = 0.106; data-to-parameter ratio = 17.2. C25H19NO2, the furyl ring is twisted by 46.3 (1) with respect to the phenylene ring bearing the amido group. The two phenylene rings (i.e. the rings connected through the –CH CH– fragment) are twisted by 59.2 (1); in the biphenylene unit, the two benzene rings are twisted by 35.5 (1). Molecules are linked by an N—HÁ Á ÁOamido hydrogen bond into a zigzag chain running along the c axis. Related literature For the use of radical cations in heterocyclic synthesis, see: Thomas et al (2004, 2008).
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