Abstract
In the title compound, C12H13N3O, the morpholine ring adopts a chair conformation and its mean plane is inclined to that of the benzene ring by 16.78 (12)°. The N—N=C—C bridge, which has an E conformation, has a torsion angle of 173.80 (19)°. In the crystal, molecules stack along the a axis but there are no significant intermolecular interactions present.
Highlights
Structure Reports OnlineKey indicators: single-crystal X-ray study; T = 296 K; mean (C–C) = 0.004 A; R factor = 0.063; wR factor = 0.094; data-to-parameter ratio = 16.4
In the title compound, C12H13N3O, the morpholine ring adopts a chair conformation and its mean plane is inclined to that of the benzene ring by 16.78 (12)
Molecules stack along the a axis but there are no significant intermolecular interactions present
Summary
Key indicators: single-crystal X-ray study; T = 296 K; mean (C–C) = 0.004 A; R factor = 0.063; wR factor = 0.094; data-to-parameter ratio = 16.4. C12H13N3O, the morpholine ring adopts a chair conformation and its mean plane is inclined to that of the benzene ring by 16.78 (12). The N—N C—C bridge, which has an E conformation, has a torsion angle of 173.80 (19). Molecules stack along the a axis but there are no significant intermolecular interactions present. Related literature For background to the importance of Schiff bases, see: Dhar & Taploo (1982); Zheng et al (2009); Guzen et al (2007); Asif (2014); Hisaindee et al (2013). See: Akkurt et al (2013)
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