Abstract
The problem of high-resolution solid state NMR of quadrupolar nuclear spins (where I> 1 2 ) has been recently solved. The twin techniques of dynamic angle spinning (DAS) and double rotation (DOR) demonstrate resolution comparable to that observed in high-resolution spectra of 13C or 15N. This presents a substantial extension as most NMR-active spins are quadrupolar. In this review we describe previous techniques, and explain why DAS and DOR yield superior results.
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