Abstract
Abstract The crystal structure of p-cumylcalix[6]arene·2.5 dimethylformamide has revealed that the compound exists in the double partial cone conformation. The DMF molecules are bound to the calixarene via hydrogen bonds. The compound crystallizes in the triclinic space group P1 with a = 17.328(3), b = 17.981(3), c = 17.040(3) A, α = 116.56(2), β = 112.42(1), γ = 76.18(2)°, and Dc = 1.165 g cm−3 for Z = 2. Refinement based on 9418 observed reflections led to a final R value of 0.08.
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