Abstract
In the presence of SnCl 4 .5H 2 O and acetic acid, a mixture of trimethylsilyl azide and tetraallyltin underwent 1,4- and subsequently 1,2-addition, respectively, with the α,β-unsaturated aldimines to give 1,3-hydroxy azides in good yields, where the hydrolysis of the intermediary imino species was found to be crucial.
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