Abstract
Abstract(S)‐3‐Hydroxy‐2,2‐dimethylcyclohexanone (2) was converted to (−)‐stypoldione (1), the ichthyotoxic and cytotoxic metabolite of the brown alga Stypopodium zonale. The present synthesis established the absolute configuration of (−)‐stypoldione as depicted in 1.
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