Abstract
Oxidizing reagents for disulfide formation of peptides are prepared from poly(ethylene glycol)polyacrylamide (PEGA) via the stepwise solid-phase peptide synthesis (method 1) or the oligomerization of N-carboxy anhydride derivatives (method 2). The oxidation of peptides 1 and 2 was carried out with resins 1a-d and 2 to give the corresponding disulfides 1′ and 2′ in 90-100% yield.
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