Abstract
Transition metal/Y zeolites have been prepared by solid state ion exchange with microwave irradiation of mechanical mixtures of VCl3, CrCl3 ⋅ 6H2O, MnCl2 ⋅ 4H2O or CoCl2 ⋅ 6H2O with NaY zeolite at 900 W in 10–20 min. The prepared transition metal/Y zeolites were characterized by X-ray diffraction (XRD), infrared spectroscopy (IR), simultaneous thermal analysis (STA) and surface area measurement (BET). Concentration of dispersed transition metal on zeolite was measured and results revealed that transition metal was dispersed and ion exchanged onto the surface of NaY zeolite.
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