Abstract
AbstractHerein, an operationally facile method for the construction of C−S bond through direct functionalization of C (sp3)−H bond adja‐cent to heteroatoms with thiols has been developed under weakly alkaline conditions. This methodology provides a convenient and efficient strategy to synthesize various aryl thioethers using a cheap and common solvent and base in moderate to good yields. The mechanistic studies indicate that a radical process is possibly involved and the sulfur radical (RS⋅) may be a reactive species during the transformations.
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