Abstract
Abstract The first electrochemical synthesis of diphenyl carbonate was accomplished using triethylamine/tetrabutylammonium perchlorate/phenol/dichloromethane or sodium phenoxide/phenol/acetonitrile electrolyte at a [PdCl2/activated carbon and vapor grown carbon fiber] anode, 1 atm CO and 25 °C. Sodium phenoxide functioned as a promoter, triethylamine, and a supporting electrolyte, tetrabutylammonium perchlorate, for the carbonylation.
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