Abstract
The mixed-valence complex [Cu II (DMF) 4][Cu 4 I(SCN) 4 (CN) 2] (DMF = N,N-dimethylformamide) has been synthesized using a direct method of interaction and characterized by X-ray crystallography. The complex consists of layers formed by polymeric [Cu 4 I (SCN) 4 (CN) 2] n 2− anionsand the [Cu II(DMF) 4] 2+ cations disposed between anionic layers.
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