Abstract
Abstract Mg2B14 prepared by reaction of high-purity Mg and B was analyzed by X-ray diffraction and Rietveld analysis. The structure refinement for space group Imam resulted in residuals Rp = 6.95% and RBragg = 3.72% with lattice parameters a = 5.9738(3) A, b = 8.1255(4) A, and c = 10.4809(5) A. AlMgB14 produced by the same method did not yield high-purity specimens.
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