Abstract
1. The authors have studied the conditions for electrochemical synthesis of the alcoholates of Ga, Sc, Y, Ge, Ti, Zr, Nb, and Ta with anodic dissolution of the metals in absolute alcohols in the presence of a base electrolyte. The optimal base electrolytes are the salts R4NBr and R4NBF4. The limits of applicability of this synthesis method are determined when various metals are used as the anode. 2. It is postulated that the primary products of anodic oxidation of the metals are alkoxyhalides, the nature of which governs the further direction of the electrode process.
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