Abstract

A new method of preparation of NbSi alloys has been provided in this article. Electro-deoxidizing mixed Nb2O5 and SiO2 small cylindrical pellets in molten CaF2 at high temperature (1500 °C) could produce homogenous NbSi alloys. And then, the cyclic voltammogram (CV) method was used to analyze the electroreduction mechanism. This effective method could shorten procedures of production of NbSi alloys and will be promising for industrial utilization.

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