Abstract
An improved method for the preparation of dialkyl phosphoroisothiocyanatidates (II) is given. These compounds (II) are labile and decompose under the influence of heat and catalysts to the corresponding alkyl thiocyanates (III). In the presence of water they hydrolyze to dialkyl hydrogenphosphates (VI) in high yield. A series of thiourea derivatives (VII) has been prepared from II and amines.
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