Abstract
Feedstock behaviour during processing via powder injection moulding (PIM) has a critical influence on the properties of the final parts. The objective of the present study is to analyze the effect of vanadium carbide (VC) addition (1, 3, 6, 10 and 14wt.% VC) on the rheological response and stability of AISI M2 high speed steel PIM feedstocks. A binder system consisting of high density polyethylene (HDPE) and paraffin wax (PW) is proposed. The effects of VC concentration, powder loading, apparent viscosity and temperature have been investigated via capillary rheometer. The feedstocks with a 14wt.% of VC, which exhibited a variable flow behaviour was discarded. The rest of the feedstocks showed a pseudoplastic behaviour which is suitable for injection moulding and in particular, those reinforced with 6 and 10wt.% of VC exhibited the best rheological responses. In order to maximize the powder loading and ensure safety conditions, the feedstocks reinforced with 6wt.% (5.9vol.%) and 10wt.% (9.8vol.%) of VC with 68vol.% of powder loading and 3wt.% (2.8vol.%) of VC with 62vol.% of powder loading were selected to continue the rheological analysis. Rheological parameters such as flow behaviour index (n), yield stress (ơy), flow activation energy (Ea) and the general mouldability index (αstv) have been analyzed for the above mentioned feedstocks and showed suitable values for the injection moulding. The green parts produced using the three feedstocks have constant weights and dimensions, good mouldability, density, shape retention and stiffness. Therefore, the developed feedstocks are suitable for PIM.
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