Abstract

The Kyropoulos (Ky) and Czochralski (Cz) methods of crystal growth are used for large-diameter single crystals. The seeding process in these methods must induce initial crystallization by initiating contact between the seed crystals and the surface of the melted material. In the Ky and Cz methods, the seeding process lays the foundation for ingot growth during the entire growth process. When any defect occurs in this process, it is likely to spread to the entire ingot. In this paper, a vision system was constructed for auto seeding and for observing the surface of the melt in the Ky method. An algorithm was developed to detect the time when the internal convection of the melt is stabilized by observing the shape of the spoke pattern on the melt material surface. Then, the vision system and algorithm were applied to the growth furnace, and the possibility of process automation was examined for sapphire growth. To confirm that the convection of the melt was stabilized, the position of the island (i.e., the center of a spoke pattern) was detected using the vision system and image processing. When the observed coordinates for the center of the island were compared with the coordinates detected from the image processing algorithm, there was an average error of 1.87 mm (based on an image with 1024 × 768 pixels).

Highlights

  • Single-crystal sapphire is a material that has high hardness, excellent chemical stability, and optical transparency in a wide range of wavelengths

  • During sapphire growth in the Ky method, images were acquired from the melt surface of the Duringmaterial sapphire growth in the Ky system, method,and images were acquired from the melt center surfacewere of the alumina using the proposed the coordinates of the stream-line alumina material using the proposed system, and After the coordinates of the caused stream-line centerand were processed through an image processing algorithm

  • The melt material convection processed through an image processing algorithm

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Summary

Introduction

Single-crystal sapphire is a material that has high hardness, excellent chemical stability, and optical transparency in a wide range of wavelengths. Due to these advantages, it is widely used in various industries including engineering, military supply, aviation, optics, and healthcare. For the growth of large-diameter single-crystal sapphire, the Kyropoulos (Ky) and Czochralski (Cz) methods are predominately used. The Cz method is a wide spread single crystal growth technique in which alumina in melted in a crucible and the seed is pulled up; the seed is simultaneously rotated after it contacts the surface of the molten metal [2]. The Ky method is mainly used for the single crystal growth of large-diameter sapphire. Though its basic growth furnace is similar to that of the

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