Abstract
A deuteron magnetic resonance study of single crystals of K+[SO3ND2]– at –78°C has shown that the deuteron quadrupole coupling constant is 207.0 ± 1.6 kHz and asymmetry parameter 0.143 ± 0.005. The maximum principal component of the electric field gradient lies within 1° of the N—D bond direction; if the two directions are assumed to coincide, the proton and deuteron magnetic resonance studies are consistent with D[graphic omitted]D = 109.2 ± 0.6° and N—D = 1.004± 0.006 A(with no motional correction), in good agreement with the neutron diffraction structure analysis.
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