Abstract

A sensitive activation technique for the determination of trace levels of oxygen in a wide range of materials is described with particular emphasis on the γ-irradiation facilities at AERE Harwell and experience of the use of the technique over a number of years. Procedures for removing surface oxygen contamination prior to determination of bulk oxygen concentrations are given, together with details of the radiochemical separation procedures used for a wide range of materials, and examples of the results obtained.

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