Abstract
The distribution of substituents in benzylated starches has been investigated by g.l.c.—m.s. of the products obtained after reductive depolymerization of the methylated polysaccharides. Reductive degradation using triethylsilane causes O-debenzylation, the degree of cleavage depending on the type of Lewis acid used. The results are discussed in comparison to those of standard methylation analysis.
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