Abstract
A method, based on X-ray absorption spectroscopy (XAS) in the range 0.8–1.5 keV, to determine the relative amounts of rare earth ions in different valencies is explained and tested for the case of terbium mixed oxides. The results are in agreement with those obtained by existing analytical methods. The XAS method is advantageous in that it can be applied where other, conventional, methods break down.
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