Abstract
Dilute solutions of transition metal ions, including copper(II), cobalt(II), nickel(II), lead(II) and iron(III), can be determined using reversed-phase liquid chromatography on Hypersil ODS by direct injection into an eluent containing sodium diethyldithiocarbamate (0.05%m/V). The complexes formed are detected using a variable wavelength detector. The effects of reagent concentration, flow-rate and pH have been examined.
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