Abstract

In this paper a novel method for determination of Fe in uranium matrix has been demonstrated using en- ergy dispersive X-ray fluorescence (EDXRF) technique. Effects of various parameters such as variation of matrix concentration, detection limit, accuracy, precision, com- parison with other established methods etc. were investi- gated in detail. Analysis of synthetic standards as well as real samples shows that for ten determinations relative standard deviation (RSD) is\2 %. The method can be used for determination of 2.24-3500 l gm L -1 Fe in uranium

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