Abstract
Abstract Numerous papers on the determination of free sulfur in rubber mixtures have been published. Most of these are in the older literature, and they offer various methods for determining free sulfur. In principle the methods can be divided into two general groups. The procedures described in the first and larger group involve preliminary acetone extraction before the actual determination of the free sulfur, whereas the methods comprising the second group, which include only two different procedures, do not involve acetone extraction. Of these two methods, only that of Oldham, Baker, and Craytor has found widespread acceptance.
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