Abstract
Capillary zone electrophoresis (CZE) was employed to separate sugars according to their electrophorectic mobilities in strong alkaline solutions (pH ca. 13). Saccharide zones were monitored electrochemically using amperometric detection at a constant potential, 0.63 V (vs Ag/AgCl), with a cylindrical copper wire electrode (25 μm in diameter). The Cu-wire microelectrode in strong basic solutions had electrochemical behavior similar to that of Cu electrodes with larger dimensions and appeared to show no deterioration for hundreds of runs
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