Abstract
A method was developed for determination of Ethinylestradiol, Diethylstilbestrol, 4-Nonylphenol and Estradiol benzoate residue in fish samples using solid phase extraction and high performance liquid chromatography. Samples were extracted and filtered for HPLC analysis. The analysis was used gradient elution with acetonitrile-water as the mobile phase. Under the optimized conditions, a method with good reproducibility (1.16%~2.45%) and the recovery (80.0%~92.5%) was developed for target components in spiked fish samples. The calibration curves were linear with correlation coefficient ranged from 0.9970 to 0.9983. The detection limit of the method was ranged from 0.0606 to 0.6066μg/ml.This method was rapid, sensitive and nothing interfered determination of the 4 kind of components.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
